Sterile formulation Checklist

                  i.            Compounding:

 

Check List:

1.       Area Temp, RH, DP

2.       Area & Equipments Cleanliness & Removal of Previous Product things

3.       CIP & SIP – Rinse Water Reports

4.       Integrities of Hydrophobic & Hydrophilic Filters

5.       Calibration of pH, Conductivity meters, Weighing Balance

6.       Availability of Hose Pipes, Silicone pipes

7.       Availability of Steam, Compressed Air/Nitrogen, Chilled Water

8.       Availability of Measuring Cylinder, Glass wares

9.       Calibration Labels with-in Due Date

10.   Integrity of vent Filter with-in Due date

11.   Preventive Maintenance Status

12.   Updation of All details ON-LINE in Log-Books

13.   Receivable Raw-Materials from WH & Weight verification.

14.   Procedure Followed As Per SOP & BMR

 

ii.            Warehouse:

 

Check List:

1.       Area Temp, RH, DP

2.       Area & Equipments Cleanliness & Removal of Previous Product things

3.       Calibration of Weighing Balance & Calibration Labels with-in Due Date

4.       Preventive Maintenance Status

5.       Updation of All details ON-LINE in Log-Books

6.       Verification of QC-Approved Label, Item code, Lot No., A.R.No of Raw material, API, Primary, Secondary packing Materials

7.       Dispensing Procedure Followed As Per SOP

 

iii.                                      Autoclave:

 

Check List:

1.       Area Temp, RH, DP

2.       Area & Equipments Cleanliness & Removal of Previous Product things

3.       Availability of Steam, Compressed Air, Strip chart.

4.       Calibration Labels with-in Due Date

5.       Integrity of vent Filter with-in Due date

6.       Preventive Maintenance Status

7.       Updation of All details ON-LINE in Log-Books

8.       Load-Pattern Procedure Followed As Per SOP


 

iv.                                       Washing &Tunnel:

 

Check List:

 

1.       Area Temp, RH, DP

2.       Area & Equipments Cleanliness & Removal of Previous Product things

3.       Calibration Labels with-in Due Date

4.       Preventive Maintenance Status

5.       Updation of All details ON-LINE in Log-Books

6.       Change Parts & Recipe selection

7.       Availability of WFI, Compressed Air

8.       Check the pressure of WFI, Re-Circulated water, Compressed Air.

9.       Check the Availability of Strip chart

10.   Tunnel Conveyer speed & Washing Machine Recipe

11.   Washing, De-Pyrogenation Procedure Followed As Per SOP

 

v.                                           Filling:

 

Check List:

 

1.       Area Temp, RH, DP

2.       Area & Equipments Cleanliness & Removal of Previous Product things

3.       Check ON-LINE particle machine should be on condition

4.       Micro-Monitoring

5.       Integrities of Hydrophobic & Hydrophilic Filters

6.       Availability of Sterilized items of Garments, Filling Change Parts, Filling Items, SS items

7.       Calibration Labels with-in Due Date

8.       Preventive Maintenance Status

9.       Updation of All details ON-LINE in Log-Books

10.   Receivable of Filtered Solution from compounding

11.   Filling Machine Recipe, Fill volume set-up & verification

12.   Procedure Followed As Per SOP

 

vi.                                     Sealing:

 

Check List:

 

1.       Area Temp, RH, DP

2.       Area & Equipments Cleanliness & Removal of Previous Product things

3.       Calibration Labels with-in Due Date

4.       Preventive Maintenance Status

5.       Updation of All details ON-LINE in Log-Books

6.       Sealing Machine Recipe, Sealing verification (Crimping, Dentate, Flip-off, Seal colour, Tightness)

7.       Procedure Followed As Per SOP


 

vii.                                    Terminal Sterilization:

 

Check List:

 

1.       Area & Equipments Cleanliness & Removal of Previous Product things

2.       Availability of Pure-Steam, Purified Water, Compressed Air, Strip chart.

3.       Calibration Labels with-in Due Date

4.       Preventive Maintenance Status

5.       Updation of All details ON-LINE in Log-Books

6.       Load-Pattern Procedure Followed As Per SOP

 

viii.                               Lyophilizer:

Check List:

 

1.       Area & Equipment’s Cleanliness & Removal of Previous Product things

2.       Availability of CIP, SIP, History data & Vacuum leak test data and Integrity data

3.       Calibration Labels with-in Due Date

4.       Preventive Maintenance Status

5.       Check the Lyophilizer recipe

6.       Updation of All details ON-LINE in Log-Books



i.                                         Packing:

Check List:

 

1.       Area Temp

2.       Area & Equipments Cleanliness & Removal of Previous Product things

3.       Calibration Labels with-in Due Date

4.       Preventive Maintenance Status

5.       Updation of All details ON-LINE in Log-Books

6.       Receivable Materials from WH

7.       Visual/Optical inspection – Low volume, High volume, White, Black, Fiber, Glass, seal rejections, others.

8.       Label Physical Verification, Labeling, Packing & weight checking

9.       Collection of Control, Stability Samples, Others sample after Packing

10.   Finally Transfer of Packing Materials /Finished goods to Warehouse

11.   Procedure Followed As Per SOP


 

ix.